40 CFR 90.317 - Carbon monoxide analyzer calibration.
(b) Initial and periodic interference. Prior to its initial use and annually thereafter, check the NDIR carbon monoxide analyzer for response to water vapor and CO2.
(1) Follow good engineering practices for instrument start-up and operation. Adjust the analyzer to optimize performance on the most sensitive range to be used.
(3) Bubble a mixture of three percent CO2 in N2 through water at room temperature and record analyzer response.
(4) An analyzer response of more than one percent of full scale for ranges above 300 ppm full scale or more than three ppm on ranges below 300 ppm full scale requires corrective action. (Use of conditioning columns is one form of corrective action which may be taken.)
(c) Initial and periodic calibration. Prior to its initial use and monthly thereafter, or within one month prior to the certification test, calibrate the NDIR carbon monoxide analyzer.
(3) Calibrate on each used operating range with carbon monoxide-in-N2 calibration gases having nominal concentrations between 10 and 90 percent of that range. A minimum of six evenly spaced points covering at least 80 percent of the 10 to 90 range (64 percent) is required (see following table).
|Example calibration points (%)||Acceptable for calibration?|
|20, 30, 40, 50, 60, 70||No, range covered is 50 percent, not 64.|
|20, 30, 40, 50, 60, 70, 80, 90||Yes.|
|10, 25, 40, 55, 70, 85||Yes.|
|10, 30, 50, 70, 90||No, though equally spaced and entire range covered, a minimum of six points are needed.|
Additional calibration points may be generated. For each range calibrated, if the deviation from a least-squares best-fit straight line is two percent or less of the value at each data point, calculate concentration values by use of a single calibration factor for that range. If the deviation exceeds two percent at any point, use the best-fit non-linear equation which represents the data to within two percent of each test point to determine concentration.
Title 40 published on 2013-07-01
no entries appear in the Federal Register after this date.