40 CFR Part 122, Appendix D to Part 122 - NPDES Permit Application Testing Requirements (

View PDF at GPO Pt. 122, App. D
Appendix D to Part 122—NPDES Permit Application Testing Requirements (§ 122.21)
Table I—Testing Requirements for Organic Toxic Pollutants by Industrial Category for Existing Dischargers
Industrial category GC/MS Fraction 1
Volatile Acid Base/neutral Pesticide
1 The toxic pollutants in each fraction are listed in Table II.
2 Testing required.
Adhesives and Sealants 2 2 2
Aluminum Forming 2 2 2
Auto and Other Laundries 2 2 2 2
Battery Manufacturing 2 2
Coal Mining 2 2 2 2
Coil Coating 2 2 2
Copper Forming 2 2 2
Electric and Electronic Components 2 2 2 2
Electroplating 2 2 2
Explosives Manufacturing 2 2
Foundries 2 2 2
Gum and Wood Chemicals 2 2 2 2
Inorganic Chemicals Manufacturing 2 2 2
Iron and Steel Manufacturing 2 2 2
Leather Tanning and Finishing 2 2 2 2
Mechanical Products Manufacturing 2 2 2
Nonferrous Metals Manufacturing 2 2 2 2
Ore Mining 2 2 2 2
Organic Chemicals Manufacturing 2 2 2 2
Paint and Ink Formulation 2 2 2 2
Pesticides 2 2 2 2
Petroleum Refining 2 2 2 2
Pharmaceutical Preparations 2 2 2
Photographic Equipment and Supplies 2 2 2 2
Plastic and Synthetic Materials Manufacturing 2 2 2 2
Plastic Processing 2
Porcelain Enameling 2 2 2
Printing and Publishing 2 2 2 2
Pulp and Paper Mills 2 2 2 2
Rubber Processing 2 2 2
Soap and Detergent Manufacturing 2 2 2
Steam Electric Power Plants 2 2 2
Textile Mills 2 2 2 2
Timber Products Processing 2 2 2 2
Table II—Organic Toxic Pollutants in Each of Four Fractions in Analysis by Gas Chromatography/Mass Spectroscopy (GS/MS)
Volatiles
1Vacrolein
2Vacrylonitrile
3Vbenzene
5Vbromoform
6Vcarbon tetrachloride
7Vchlorobenzene
8Vchlorodibromomethane
9Vchloroethane
10V2-chloroethylvinyl ether
11Vchloroform
12Vdichlorobromomethane
14V1,1-dichloroethane
15V1,2-dichloroethane
16V1,1-dichloroethylene
17V1,2-dichloropropane
18V1,3-dichloropropylene
19Vethylbenzene
20Vmethyl bromide
21Vmethyl chloride
22Vmethylene chloride
23V1,1,2,2-tetrachloroethane
24Vtetrachloroethylene
25Vtoluene
26V1,2-trans-dichloroethylene
27V1,1,1-trichloroethane
28V1,1,2-trichloroethane
29Vtrichloroethylene
31Vvinyl chloride
Acid Compounds
1A2-chlorophenol
2A2,4-dichlorophenol
3A2,4-dimethylphenol
4A4,6-dinitro-o-cresol
5A2,4-dinitrophenol
6A2-nitrophenol
7A4-nitrophenol
8Ap-chloro-m-cresol
9Apentachlorophenol
10Aphenol
11A2,4,6-trichlorophenol
Base/Neutral
1Bacenaphthene
2Bacenaphthylene
3Banthracene
4Bbenzidine
5Bbenzo(a)anthracene
6Bbenzo(a)pyrene
7B3,4-benzofluoranthene
8Bbenzo(ghi)perylene
9Bbenzo(k)fluoranthene
10Bbis(2-chloroethoxy)methane
11Bbis(2-chloroethyl)ether
12Bbis(2-chloroisopropyl)ether
13Bbis (2-ethylhexyl)phthalate
14B4-bromophenyl phenyl ether
15Bbutylbenzyl phthalate
16B2-chloronaphthalene
17B4-chlorophenyl phenyl ether
18Bchrysene
19Bdibenzo(a,h)anthracene
20B1,2-dichlorobenzene
21B1,3-dichlorobenzene
22B1,4-dichlorobenzene
23B3,3′-dichlorobenzidine
24Bdiethyl phthalate
25Bdimethyl phthalate
26Bdi-n-butyl phthalate
27B2,4-dinitrotoluene
28B2,6-dinitrotoluene
29Bdi-n-octyl phthalate
30B1,2-diphenylhydrazine (as azobenzene)
31Bfluroranthene
32Bfluorene
33Bhexachlorobenzene
34Bhexachlorobutadiene
35Bhexachlorocyclopentadiene
36Bhexachloroethane
37Bindeno(1,2,3-cd)pyrene
38Bisophorone
39Bnapthalene
40Bnitrobenzene
41BN-nitrosodimethylamine
42BN-nitrosodi-n-propylamine
43BN-nitrosodiphenylamine
44Bphenanthrene
45Bpyrene
46B1,2,4-trichlorobenzene
Pesticides
1Paldrin
2Palpha-BHC
3Pbeta-BHC
4Pgamma-BHC
5Pdelta-BHC
6Pchlordane
7P4,4′-DDT
8P4,4′-DDE
9P4,4′-DDD
10Pdieldrin
11Palpha-endosulfan
12Pbeta-endosulfan
13Pendosulfan sulfate
14Pendrin
15Pendrin aldehyde
16Pheptachlor
17Pheptachlor epoxide
18PPCB-1242
19PPCB-1254
20PPCB-1221
21PPCB-1232
22PPCB-1248
23PPCB-1260
24PPCB-1016
25Ptoxaphene
Table III—Other Toxic Pollutants (Metals and Cyanide) and Total Phenols
Antimony, Total
Arsenic, Total
Beryllium, Total
Cadmium, Total
Chromium, Total
Copper, Total
Lead, Total
Mercury, Total
Nickel, Total
Selenium, Total
Silver, Total
Thallium, Total
Zinc, Total
Cyanide, Total
Phenols, Total
Table IV—Conventional and Nonconventional Pollutants Required To Be Tested by Existing Dischargers if Expected to be Present
Bromide
Chlorine, Total Residual
Color
Fecal Coliform
Fluoride
Nitrate-Nitrite
Nitrogen, Total Organic
Oil and Grease
Phosphorus, Total
Radioactivity
Sulfate
Sulfide
Sulfite
Surfactants
Aluminum, Total
Barium, Total
Boron, Total
Cobalt, Total
Iron, Total
Magnesium, Total
Molybdenum, Total
Manganese, Total
Tin, Total
Titanium, Total
Table V—Toxic Pollutants and Hazardous Substances Required To Be Identified by Existing Dischargers if Expected To Be Present
Toxic Pollutants
Asbestos
Hazardous Substances
Acetaldehyde
Allyl alcohol
Allyl chloride
Amyl acetate
Aniline
Benzonitrile
Benzyl chloride
Butyl acetate
Butylamine
Captan
Carbaryl
Carbofuran
Carbon disulfide
Chlorpyrifos
Coumaphos
Cresol
Crotonaldehyde
Cyclohexane
2,4-D (2,4-Dichlorophenoxy acetic acid)
Diazinon
Dicamba
Dichlobenil
Dichlone
2,2-Dichloropropionic acid
Dichlorvos
Diethyl amine
Dimethyl amine
Dintrobenzene
Diquat
Disulfoton
Diuron
Epichlorohydrin
Ethion
Ethylene diamine
Ethylene dibromide
Formaldehyde
Furfural
Guthion
Isoprene
Isopropanolamine Dodecylbenzenesulfonate
Kelthane
Kepone
Malathion
Mercaptodimethur
Methoxychlor
Methyl mercaptan
Methyl methacrylate
Methyl parathion
Mevinphos
Mexacarbate
Monoethyl amine
Monomethyl amine
Naled
Napthenic acid
Nitrotoluene
Parathion
Phenolsulfanate
Phosgene
Propargite
Propylene oxide
Pyrethrins
Quinoline
Resorcinol
Strontium
Strychnine
Styrene
2,4,5-T (2,4,5-Trichlorophenoxy acetic acid)
TDE (Tetrachlorodiphenylethane)
2,4,5-TP [2-(2,4,5-Trichlorophenoxy) propanoic acid]
Trichlorofan
Triethanolamine dodecylbenzenesulfonate
Triethylamine
Trimethylamine
Uranium
Vanadium
Vinyl acetate
Xylene
Xylenol
Zirconium
[Note 1: The Environmental Protection Agency has suspended the requirements of § 122.21(g)(7)(ii)(A) and Table I of Appendix D as they apply to certain industrial categories. The suspensions are as follows:
a. At 46 FR 2046, Jan. 8, 1981, the Environmental Protection Agency suspended until further notice § 122.21(g)(7)(ii)(A) as it applies to coal mines.
b. At 46 FR 22585, Apr. 20, 1981, the Environmental Protection Agency suspended until further notice § 122.21(g)(7)(ii)(A) and the corresponding portions of Item V-C of the NPDES application Form 2c as they apply to:
1. Testing and reporting for all four organic fractions in the Greige Mills Subcategory of the Textile Mills industry (Subpart C—Low water use processing of 40 CFR part 410), and testing and reporting for the pesticide fraction in all other subcategories of this industrial category.
2. Testing and reporting for the volatile, base/neutral and pesticide fractions in the Base and Precious Metals Subcategory of the Ore Mining and Dressing industry (subpart B of 40 CFR part 440), and testing and reporting for all four fractions in all other subcategories of this industrial category.
3. Testing and reporting for all four GC/MS fractions in the Porcelain Enameling industry.
c. At 46 FR 35090, July 1, 1981, the Environmental Protection Agency suspended until further notice § 122.21(g)(7)(ii)(A) and the corresponding portions of Item V-C of the NPDES application Form 2c as they apply to:
1. Testing and reporting for the pesticide fraction in the Tall Oil Rosin Subcategory (subpart D) and Rosin-Based Derivatives Subcategory (subpart F) of the Gum and Wood Chemicals industry (40 CFR part 454), and testing and reporting for the pesticide and base/netural fractions in all other subcategories of this industrial category.
2. Testing and reporting for the pesticide fraction in the Leather Tanning and Finishing, Paint and Ink Formulation, and Photographic Supplies industrial categories.
3. Testing and reporting for the acid, base/neutral and pesticide fractions in the Petroleum Refining industrial category.
4. Testing and reporting for the pesticide fraction in the Papergrade Sulfite subcategories (subparts J and U) of the Pulp and Paper industry (40 CFR part 430); testing and reporting for the base/neutral and pesticide fractions in the following subcategories: Deink (subpart Q), Dissolving Kraft (subpart F), and Paperboard from Waste Paper (subpart E); testing and reporting for the volatile, base/neutral and pesticide fractions in the following subcategories: BCT Bleached Kraft (subpart H), Semi-Chemical (subparts B and C), and Nonintegrated-Fine Papers (subpart R); and testing and reporting for the acid, base/neutral, and pesticide fractions in the following subcategories: Fine Bleached Kraft (subpart I), Dissolving Sulfite Pulp (subpart K), Groundwood-Fine Papers (subpart O), Market Bleached Kraft (subpart G), Tissue from Wastepaper (subpart T), and Nonintegrated-Tissue Papers (subpart S).
5. Testing and reporting for the base/neutral fraction in the Once-Through Cooling Water, Fly Ash and Bottom Ash Transport Water process wastestreams of the Steam Electric Power Plant industrial category.
This revision continues these suspensions.]*

Footnote(s):
* Editorial Note: The words “This revision” refer to the document published at 48 FR 14153, Apr. 1, 1983.

For the duration of the suspensions, therefore, Table I effectively reads:
Table I—Testing Requirements for Organic Toxic Pollutants by Industry Category
Industry category GC/MS fraction 2
Volatile Acid Neutral Pesticide
1 Testing required.
2 The pollutants in each fraction are listed in Item V-C.
3 Pulp and Paperboard Mills:
Adhesives and sealants (1) (1) (1)
Aluminum forming (1) (1) (1)
Auto and other laundries (1) (1) (1) (1)
Battery manufacturing (1) (1)
Coal mining
Coil coating (1) (1) (1)
Copper forming (1) (1) (1)
Electric and electronic compounds (1) (1) (1) (1)
Electroplating (1) (1) (1)
Explosives manufacturing (1) (1)
Foundries (1) (1) (1)
Gum and wood (all subparts except D and F) (1) (1)
Subpart D—tall oil rosin (1) (1) (1)
Subpart F—rosin-based derivatives (1) (1) (1)
Inorganic chemicals manufacturing (1) (1) (1)
Iron and steel manufacturing (1) (1) (1)
Leather tanning and finishing (1) (1) (1)
Mechanical products manufacturing (1) (1) (1)
Nonferrous metals manufacturing (1) (1) (1) (1)
Ore mining (applies to the base and precious metals/Subpart B) (1)
Organic chemicals manufacturing (1) (1) (1) (1)
Paint and ink formulation (1) (1) (1)
Pesticides (1) (1) (1) (1)
Petroleum refining (1)
Pharmaceutical preparations (1) (1) (1)
Photographic equipment and supplies (1) (1) (1)
Plastic and synthetic materials manufacturing (1) (1) (1) (1)
Plastic processing (1)
Porcelain enameling
Printing and publishing (1) (1) (1) (1)
Pulp and paperboard mills—see footnote 3
Rubber processing (1) (1) (1)
Soap and detergent manufacturing (1) (1) (1)
Steam electric power plants (1) (1)
Textile mills (Subpart C—Greige Mills are exempt from this table) (1) (1) (1)
Timber products processing (1) (1) (1) (1)
Subpart 3 GS/MS fractions
VOA Acid Base/neutral Pesticides
1 Must test.
2 Do not test unless “reason to believe” it is discharged.
3 Subparts are defined in 40 CFR Part 430.
A 2 (1) 2 (1)
B 2 (1) 2 2
C 2 (1) 2 2
D 2 (1) 2 2
E (1) (1) 2 (1)
F (1) (1) 2 2
G (1) (1) 2 2
H (1) (1) 2 2
I (1) (1) 2 2
J (1) (1) (1) 2
K (1) (1) 2 2
L (1) (1) 2 2
M (1) (1) 2 2
N (1) (1) 2 2
O (1) (1) 2 2
P (1) (1) 2 2
Q (1) (1) 2 (1)
R 2 (1) 2 2
S (1) (1) 2 (1)
T (1) (1) 2 (1)
U (1) (1) (1) 2
[48 FR 14153, Apr. 1, 1983, as amended at 49 FR 38050, Sept. 26, 1984; 50 FR 6940, Feb. 19, 1985]

Title 40 published on 2013-07-01

no entries appear in the Federal Register after this date.

Title 40 published on 2013-07-01

The following are ALL rules, proposed rules, and notices (chronologically) published in the Federal Register relating to 40 CFR 122 after this date.

  • 2014-06-24; vol. 79 # 121 - Tuesday, June 24, 2014
    1. 79 FR 35712 - Definition of “Waters of the United States” Under the Clean Water Act; Extension of Comment Period
      GPO FDSys XML | Text
      ENVIRONMENTAL PROTECTION AGENCY, DEPARTMENT OF DEFENSE, Department of the Army, Corps of Engineers
      Proposed rule; Extension of Comment Period.
      Comments must be received on or before October 20, 2014. The comment period was originally scheduled to end on July 21, 2014.
      33 CFR Part 328