Iowa Admin. Code r. 567-41.8 - Radionuclides.
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15 pCi/L |
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Combined Radium-226 and Radium-228 |
5 pCi/Li |
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Uranium |
30 µg/L |
1The combined radium-226 and radium-228 value is determined by the addition of the results of the analysis for radium-226 and the analysis for radium-228.
Average Annual Concentrations Assumed to Produce a Total Body or Organ Dose of 4 mrem/year
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Radionuclide |
Critical Organ |
Concentration |
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Strontium-90 |
Bone marrow |
8 pCi/L |
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Tritium |
Total body |
20,000 pCi/L |
Detection Limits for
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Detection Limit |
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3 pCi/L |
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Radium-226 |
1 pCi/L |
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Radium-228 |
1 pCi/L |
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Uranium |
1 µg/L |
Detection Limits for
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Detection Limit |
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Gross beta |
4 pCi/L |
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Cesium-134 |
10 pCi/L |
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Iodine-131 |
1 pCi/L |
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Strontium-89 |
10 pCi/L |
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Strontium-90 |
2 pCi/L |
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Tritium |
1,000 pCi/L |
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Other radionuclides |
1/10 of the applicable limit |
RADIONUCLIDE ANALYTICAL METHODOLOGY
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Methodology |
Reference (method or page number) |
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EPA1 |
EPA2 |
EPA3 |
EPA4 |
SM5 |
ASTM6 |
USGS7 |
DOE8 |
Other |
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Naturally occurring |
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Gross alpha11 & beta |
Evaporation |
900 0 |
P 1 |
00-01 |
P. 1 |
302, 7110B, 7110 B-00 |
R-1120-76 |
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Gross alpha11 |
Co-precipitation |
00-02 |
7110C, 7110C-00 |
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Radium-226 |
Radon emanation |
903 1 |
p 16 |
Ra-04 |
p. 19 |
305, 7500-Ra C, 7500RaC-01 |
D 3454-97, 05 |
R-1141-76 |
Ra-04 |
NY9 |
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Radiochemical |
903 0 |
p 13 |
Ra-03 |
304, 7500-Ra B, 7500-Ra B-01 |
D 2460-97, 07 |
R-1140-76 |
GA14 |
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Radium-228 |
Radiochemical |
904 0 |
p 24 |
Ra-05 |
p. 19 |
7500-Ra D, 7500-Ra D-01 |
R-1142-76 |
NY9 NJ10 GA14 |
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Uranium12 |
Radiochemical |
908 0 |
7500-U B, 7500-U B-00 |
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Fluorometnc ICP-MS |
908 1 200 813 |
7500-U C (17th edition) 3125 |
D 2907-97 D 5673-03, 05, 10 |
R-1180-76 R-1181-76 |
U-04 |
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Alpha spectrometry |
00-07 |
p. 33 |
7500-U C, 7500-U C-00 |
D 3972-97, 02,09 |
R-1182-76 |
U-02 |
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Laser phosphonmetry |
D 5174-97, 02,07 |
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Alpha liquid scintillation spectrometry |
D 6239-09 |
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Man-made |
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Radioactive Cesium |
Radiochemical |
9010 |
P 4 |
7500-Cs B, 7500-Cs B-00 |
D 2459-72 |
R-llll-76 |
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Gamma ray spectrometry |
901.1 |
p. 92 |
7120, 7120-97 |
D 3649-91, 98a, 06 |
R-1110-76 |
4.5.2.3 |
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Radioactive Iodine |
Radiochemical |
902.0 |
p. 6 p. 9 |
7500-I B, 7500-I B-00 7500-I C, 7500-I C-00 7500-I D, 7500-I D-00 |
D 3649-91, 98a, 06 |
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Gamma ray spectrometry |
901.1 |
p. 92 |
7120, 7120-97 |
D 4785-93, 00a, 08 |
4.5.2.3 |
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Radioactive Strontium 89, 90 |
Radiochemical |
905.0 |
p. 29 |
Sr-04 |
p. 65 |
303, 7500-Sr B, 7500-SrB-01 |
R-1160-76 |
Sr-01 Sr-02 |
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Tritium |
Liquid scintillation |
906.0 |
p. 34 |
H-02 |
p. 87 |
306, 7500-3H B, 7500-3H B-00 |
D 4107-91, 98 (Reapproved 2002), 08 |
R-1171-76 |
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Gamma emitters |
Gamma ray spectrometry |
901.1 902.0 901.0 |
p. 92 |
7120 7500-Cs B, 7500-Cs B-00 7500-I B, 7500-I B-00 |
D 3649-91, 98a, 06 D 4785-93, 00a, 08 |
R-1110-76 |
Ga-01-R |
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The procedures shall be done in accordance with the
documents listed below. The incorporation by reference of documents 1 through
10 was approved by the
1Prescribed Procedures for
Measurement of Radioactivity in Drinking Water," EPA 600/4-80-032, August 1980.
Available at the US
2"Interim Radiochemical Methodology for Drinking Water," EPA 600/4-75-008(revised), March 1976. Available at NTIS, ibid. PB 253258.
3"Radiochemistry Procedures Manual," EPA 520/5-84-006, December 1987. Available at NTIS, ibid. PB 84-215581.
4Radiochemical Analytical Procedures for Analysis of Environmental Samples," March 1979. Available at NTIS, ibid. EMSL LV 053917.
5
6Annual Book of ASTM Standards, Volumes 11.01 and 11.02, 2002. Any year containing the cited version of the method may be used. Available at ASTM International, 100 Barr Harbor Drive, West Conshohocken, PA 19428.
7"Methods for Determination of Radioactive Substances in Water and Fluvial Sediments," Chapter A5 in Book 5 of Techniques of Water-Resources Investigations of the United States Geological Survey, 1977. Available at U.S. Geological Survey (USGS) Information Services, Box 25286, Federal Center, Denver, CO 80225-0425.
8"EML Procedures Manual," 28th
(1997) or 27th (1990) edition, Volumes 1 and 2; either edition may be used. In
the 27th edition, Method Ra-04 is listed as Ra-05, and Method Ga-01-R is listed
as Sect. 4.5.2.3. Available at the Environmental Measurements Laboratory, U.S.
9Determination of Ra-226 and
Ra-228 (Ra-02)," January 1980, revised June 1982. Available at Radiological
Sciences Institute Center for Laboratories and Research, New York State
10Determination of Radium-228 in
Drinking Water," August 1980. Available at State of New Jersey,
11Natural uranium and thorium-230 are approved as gross alpha calibration standards for gross alpha with co-precipitation and evaporation methods; americium-241 is approved with co-precipitation methods.
12If uranium (U) is determined by mass, a 0.67 pCi/ng of uranium conversion factor must be used. This conversion factor is based on the 1:1 activity ratio of U-234 to U-238 that is characteristic of naturally occurring uranium.
13Determination of Trace Elements in Waters and Wastes by Inductively Coupled Plasma-Mass Spectrometry," Revision 5.4, which is published in "Methods for the Determination of Metals in Environmental Samples - Supplement 1," EPA 600-R-94-111, May 1994. Available at NTIS, PB 95-125472.
14"The Determination of Radium-226 and Radium-228 in Drinking Water by Gamma-Ray Spectrometry Using HPGW or Ge(Li) Detectors," Revision 1.2, December 2004. Available from Environmental Resources Center, Georgia Institute of Technology, 620 Cherry Street, Atlanta, GA 30332-0335; telephone: (404)894-3776.
*
* Iodine-131. A composite of five consecutive daily samples
shall be analyzed once each quarter for iodine-131. The
* Strontium-90 and tritium. Annual monitoring for strontium-90 and tritium shall be conducted by means of the analysis of a composite of four consecutive quarterly samples or analysis of four quarterly samples. The latter procedure is recommended.
Notes
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